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Advanced Analytical Services

Pyroprobe 5200HPR

CDS has introduced the first and only high-pressure pyrolysis system. Scientists studying new material, such as various biomass feed stock, need to understand how these materials break down in a reactor at varying conditions. The high-pressure pyrolyzer allows them to study both high temperature & pressure on a small scale in the lab before undergoing the time and expense of scaling up to a pilot reactor. And in addition, the background gas can be carrier gas or a reactant gas such as air or oxygen.

The High Pressure Pyrolysis instrument will use the model 5200 which has been modified with a back pressure regulator (BPR) to the trap of the 5200. Samples can then be pyrolyzed at elevated pressures (500PSI max) and collected onto the built-in trap. After pyrolysis of the sample is complete, the analytes can be transferred to the GC at normal operating conditions. Any reactant gas can be used including H2, O2, CH4 or CO in the pyrolysis chamber.

 

Compatible with all GC makes and models.

Uses a resistively heated element utilizing a coiled platinum filament for variable temperature control. This allows for fast and slow pyrolysis-heating rates that shall be programmable in degrees per millisecond, in degrees per second, and in degrees per minute.

Optional Catalyst Reactor

  • Heated Tubular Reactor: Includes independently temperature controlled reactor zone (800°C) between the Pyroprobe and the back-pressure regulator of the High-Pressure 5200. Catalyst for the reactor is contained in easily removable stainless steel tubes. Volatiles produced by pyrolysis are carried through the reactor, and the resulting products are collected onto the trap of the Pyroprobe, for transfer to a GC or GC/MS for analysis.

 

Analysis of Acrylate Polymers by Direct Pyrolysis-FT-IR.pdf Analysis of Photocopier Toners by Pyrolysis-FT-IR.pdf Analysis of Poly (vinyl chloride) by Direct Pyrolysis FT-IR.pdf Analysis of Polyolefins by Pyrolysis Gas Chromatography.pdf Analytical Pyrolysis of Surfactants.pdf Capillary Gas Chromatography of Polyolefin Pyrolysates.pdf Degradation Mechanisms-Depolymerization.pdf Degradation Mechanisms-Random Scission.pdf Degradation Mechanisms-Side Group Elimination.pdf Direct Pyrolysis-FT-IR. An Alternative Sampling System.pdf Dynamic Headspace and Pyrolysis in Ink Analysis.pdf Epoxy and Polycarbonate.pdf Evolved Gas Analysis of a Polyurethane Foam.pdf Evolved Gas Analysis of Polymers.pdf On-Column Cryofocusing for Improved Sensitivity Using Cryogenic Focusing.pdf Parameter Optimization in Pyrolysis-FT-IR.pdf Pyrolysis Gas Chromatography of Amino Acids.pdf Pyrolysis and FGA of Polyvinyl Alcohol.pdf Pyrolysis GC-MS of Biodegradable Plastic Packaging.pdf Pyrolysis of Fluoropolymers Polyvinyl Fluoride vs. Polyvinylidine Fluoride.pdf Pyrolysis of Synthetic Polymers-Improved Sensitivity Using Cryogenic Focusing.pdf Pyrolysis-FT-IR of Carbon-Filled Rubbers.pdf Pyrolysis-GC of Carbon-Filled Rubbers.pdf Pyrolysis-GC of High and Low Density Polyethlene.pdf Pyrolysis-GC of Polyolefins.pdf Pyrolysis-GC-MS of Power Coatings.pdf Pyrolysis-MSD for Rapid Polymer Analysis.pdf Pyrolytic Injection Inlet Autosampling System for the Analysis of Polymer Samples,.pdf Quantitation of Ethylene-Propylene Copolymers.pdf Quantitation of Low Levels of Methyl Methacrylate in a Copolymer.pdf Quantitative Determination of Poly (propylene-1-butene).pdf Quantitation of Epoxy to Hardener Ratios in a Cycloaliphatic Epoxy.pdf Quantitative Pyrolysis-GC in the Analysis of Copolymers.pdf Thermal Degradation of Polymers in Air.pdf Two-Step Polymer Analysis.pdf Using a Thermal Technique to Extract Residual Oligomers.pdf

Air freshener fragrances using Pyroprobe Microtrap.pdf Analysis of a Layered Paint Sample using Pyrotomy.pdf Analysis of Algae using Pyrolysis and THM.pdf Analysis of Cosmetics by Pyrolysis-GC-MS.pdf Analysis of Vulcanized Rubber by Pyrolysis-GC-MS,.pdf Antioxidant Detection in Petroleum Wax.pdf Biochemical Analysis by Pyrolysis-GC-MS.pdf Brominated Flame Retardant in PET.pdf Brominated Flame Retardants in a Polycarbonate.pdf Cracking Products of Oleic Acid and Olive Oil.pdf Detecting Differences in PEEK Preparation.pdf Four-Step Analysis of Smokeless Tobacco.pdf GC-MS of Plant Material.pdf GC-MS of Switchgrass.pdf Multi-step Analysis of Packaging Tape.pdf Multi-step Pyrolysis-GC-MS Analysis of a PVC Copolymer.pdf Pyrolysis Autosampling Reproducibility.pdf Pyrolysis GC-MS of Plant Derived (Cellulosic) Textiles.pdf Pyrolysis GC-MS to Characterize Artificial Sweeteners.pdf Pyrolysis of Fiber Blends.pdf Pyrolysis of Rubber with Antioxidant 6-PPD.pdf Pyrolysis of Soy Clothing Fiber.pdf Pyrolysis of Tobacco in Air.pdf Pyrolysis-GC-MS of Polyurethanes.pdf Pyrolysis-GC-MS of Tobacco with Menthol.pdf Tri-Step Analysis of a Latex Glove.pdf Tri-Step Analysis of Chewing Gum.pdf Injections using Pyroprobe.pdf Evaluation of Source Rock using EGA and Pyrolysis GCMS.pdf Py-GC HR-TOF of Circuit Board Polymer.pdf Pyrolysis and Reactant Gas to Detect and Study Antimicrobial Agents.pdf Pyrolysis of Coal Under Steam and Elevated Pressure PYGC.pdf Detection of Polymers Dissolved in Sea Water.pdf EGA and the Identication of a Clear Polymer.pdf Multi-Step Analysis of Automobile Tire Rubber.pdf Multi-Step Analysis of Coal by Pyrolysis-GC_MS.pdf